TY - JOUR
T1 - Crystal structure of 2,4-dimethyl-1,2,4-thiadiazolidine-3,5-dithione
AU - Raston, Colin L.
AU - White, Allan H.
AU - Willis, Anthony C.
AU - Varghese, Jose N.
PY - 1974
Y1 - 1974
N2 - The crystal structure of the title compound has been determined from X-ray diffraciometer data and refined by least squares to R 0.035 (749 reflections). Crystals are monoclinic, P21/n, a = 7.812(1), b = 15.276(3), c = 6.271-(2) Å, β = 96.41(1)°, 2 = 4. The non-hydrogen atom geometry of the planar system has been corrected throughout for thermal motion ; the conjugation is extensive throughout the S·CS·N·CS·N part of the ring but not in the N-S bond. Considerable repulsion distorts the geometry of the peripheral sulphur and methyl groups.
AB - The crystal structure of the title compound has been determined from X-ray diffraciometer data and refined by least squares to R 0.035 (749 reflections). Crystals are monoclinic, P21/n, a = 7.812(1), b = 15.276(3), c = 6.271-(2) Å, β = 96.41(1)°, 2 = 4. The non-hydrogen atom geometry of the planar system has been corrected throughout for thermal motion ; the conjugation is extensive throughout the S·CS·N·CS·N part of the ring but not in the N-S bond. Considerable repulsion distorts the geometry of the peripheral sulphur and methyl groups.
UR - http://www.scopus.com/inward/record.url?scp=5844279129&partnerID=8YFLogxK
U2 - 10.1039/P29740001096
DO - 10.1039/P29740001096
M3 - Article
AN - SCOPUS:5844279129
SN - 1472-779X
SP - 1096
EP - 1098
JO - Journal of the Chemical Society, Perkin Transactions 2
JF - Journal of the Chemical Society, Perkin Transactions 2
IS - 10
ER -