Abstract
The crystal structure of the title compound has been determined from X-ray diffraciometer data and refined by least squares to R 0.035 (749 reflections). Crystals are monoclinic, P21/n, a = 7.812(1), b = 15.276(3), c = 6.271-(2) Å, β = 96.41(1)°, 2 = 4. The non-hydrogen atom geometry of the planar system has been corrected throughout for thermal motion ; the conjugation is extensive throughout the S·CS·N·CS·N part of the ring but not in the N-S bond. Considerable repulsion distorts the geometry of the peripheral sulphur and methyl groups.
Original language | English |
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Pages (from-to) | 1096-1098 |
Number of pages | 3 |
Journal | Journal of the Chemical Society, Perkin Transactions 2 |
Issue number | 10 |
DOIs | |
Publication status | Published - 1974 |
Externally published | Yes |