Crystal structure of 3, 3a΄, 5, 5΄-tetra-t-butyl- 2΄-(3, 5-di-t-butyl-4-hydroxyphenyl)- 7΄-[l-(3, 5-di-t-butyl-4-hydroxyphenyl)ethylidene]- 3a΄, 4΄, 7΄, 7a΄-tetrahydrospiro[cyclohexa- 2, 5-diene-1, 1΄-[1h]indene]-4, 4΄-dione

Sydney R. Hall, Colin L. Raston, Allan H. White

Research output: Contribution to journalArticle

2 Citations (Scopus)

Abstract

The crystal structure of the title compound, C60H86O4, has been determined at 295 K by single crystal X-ray diffraction and refined by least squares to a residual of 0·073 for 3399 ‘observed’ reflections. Crystals are monoclinic, P21/n, a 18·999(10), b 12·149(7), c 27·589(10) Å, β 107·32(6)°, Z 4. The compound is solvated with ether to the extent of about two solvent molecules per unit cell.

Original languageEnglish
Pages (from-to)295-302
Number of pages8
JournalAustralian Journal of Chemistry
Volume33
Issue number2
DOIs
Publication statusPublished - 1980
Externally publishedYes

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