Crystal structure of 3, 3a΄, 5, 5΄-tetra-t-butyl- 2΄-(3, 5-di-t-butyl-4-hydroxyphenyl)- 7΄-[l-(3, 5-di-t-butyl-4-hydroxyphenyl)ethylidene]- 3a΄, 4΄, 7΄, 7a΄-tetrahydrospiro[cyclohexa- 2, 5-diene-1, 1΄-[1h]indene]-4, 4΄-dione

Sydney R. Hall; Colin L. Raston; Allan H. White

doi:10.1071/CH9800295

Crystal structure of 3, 3a΄, 5, 5΄-tetra-t-butyl- 2΄-(3, 5-di-t-butyl-4-hydroxyphenyl)- 7΄-[l-(3, 5-di-t-butyl-4-hydroxyphenyl)ethylidene]- 3a΄, 4΄, 7΄, 7a΄-tetrahydrospiro[cyclohexa- 2, 5-diene-1, 1΄-[1h]indene]-4, 4΄-dione

Sydney R. Hall
, Colin L. Raston
, Allan H. White

Research output: Contribution to journal › Article › peer-review

2 Citations (Scopus)

Abstract

The crystal structure of the title compound, C₆₀H₈₆O₄, has been determined at 295 K by single crystal X-ray diffraction and refined by least squares to a residual of 0·073 for 3399 ‘observed’ reflections. Crystals are monoclinic, P2₁/n, a 18·999(10), b 12·149(7), c 27·589(10) Å, β 107·32(6)°, Z 4. The compound is solvated with ether to the extent of about two solvent molecules per unit cell.

Original language	English
Pages (from-to)	295-302
Number of pages	8
Journal	Australian Journal of Chemistry
Volume	33
Issue number	2
DOIs	https://doi.org/10.1071/CH9800295
Publication status	Published - 1980
Externally published	Yes

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@article{b67734ce504147799a8536fd91085fbb,

title = "Crystal structure of 3, 3a΄, 5, 5΄-tetra-t-butyl- 2΄-(3, 5-di-t-butyl-4-hydroxyphenyl)- 7΄-[l-(3, 5-di-t-butyl-4-hydroxyphenyl)ethylidene]- 3a΄, 4΄, 7΄, 7a΄-tetrahydrospiro[cyclohexa- 2, 5-diene-1, 1΄-[1h]indene]-4, 4΄-dione",

abstract = "The crystal structure of the title compound, C60H86O4, has been determined at 295 K by single crystal X-ray diffraction and refined by least squares to a residual of 0·073 for 3399 {\textquoteleft}observed{\textquoteright} reflections. Crystals are monoclinic, P21/n, a 18·999(10), b 12·149(7), c 27·589(10) {\AA}, β 107·32(6)°, Z 4. The compound is solvated with ether to the extent of about two solvent molecules per unit cell.",

author = "Hall, \{Sydney R.\} and Raston, \{Colin L.\} and White, \{Allan H.\}",

year = "1980",

doi = "10.1071/CH9800295",

language = "English",

volume = "33",

pages = "295--302",

journal = "Australian Journal of Chemistry",

issn = "0004-9425",

publisher = "CSIRO Publishing",

number = "2",

}

Hall, SR, Raston, CL & White, AH 1980, 'Crystal structure of 3, 3a΄, 5, 5΄-tetra-t-butyl- 2΄-(3, 5-di-t-butyl-4-hydroxyphenyl)- 7΄-[l-(3, 5-di-t-butyl-4-hydroxyphenyl)ethylidene]- 3a΄, 4΄, 7΄, 7a΄-tetrahydrospiro[cyclohexa- 2, 5-diene-1, 1΄-[1h]indene]-4, 4΄-dione', Australian Journal of Chemistry, vol. 33, no. 2, pp. 295-302. https://doi.org/10.1071/CH9800295

Crystal structure of 3, 3a΄, 5, 5΄-tetra-t-butyl- 2΄-(3, 5-di-t-butyl-4-hydroxyphenyl)- 7΄-[l-(3, 5-di-t-butyl-4-hydroxyphenyl)ethylidene]- 3a΄, 4΄, 7΄, 7a΄-tetrahydrospiro[cyclohexa- 2, 5-diene-1, 1΄-[1h]indene]-4, 4΄-dione. / Hall, Sydney R.; Raston, Colin L.; White, Allan H.
In: Australian Journal of Chemistry, Vol. 33, No. 2, 1980, p. 295-302.

Research output: Contribution to journal › Article › peer-review

TY - JOUR

T1 - Crystal structure of 3, 3a΄, 5, 5΄-tetra-t-butyl- 2΄-(3, 5-di-t-butyl-4-hydroxyphenyl)- 7΄-[l-(3, 5-di-t-butyl-4-hydroxyphenyl)ethylidene]- 3a΄, 4΄, 7΄, 7a΄-tetrahydrospiro[cyclohexa- 2, 5-diene-1, 1΄-[1h]indene]-4, 4΄-dione

AU - Hall, Sydney R.

AU - Raston, Colin L.

AU - White, Allan H.

PY - 1980

Y1 - 1980

N2 - The crystal structure of the title compound, C60H86O4, has been determined at 295 K by single crystal X-ray diffraction and refined by least squares to a residual of 0·073 for 3399 ‘observed’ reflections. Crystals are monoclinic, P21/n, a 18·999(10), b 12·149(7), c 27·589(10) Å, β 107·32(6)°, Z 4. The compound is solvated with ether to the extent of about two solvent molecules per unit cell.

AB - The crystal structure of the title compound, C60H86O4, has been determined at 295 K by single crystal X-ray diffraction and refined by least squares to a residual of 0·073 for 3399 ‘observed’ reflections. Crystals are monoclinic, P21/n, a 18·999(10), b 12·149(7), c 27·589(10) Å, β 107·32(6)°, Z 4. The compound is solvated with ether to the extent of about two solvent molecules per unit cell.

UR - https://www.scopus.com/pages/publications/84970564794

U2 - 10.1071/CH9800295

DO - 10.1071/CH9800295

M3 - Article

AN - SCOPUS:84970564794

SN - 0004-9425

VL - 33

SP - 295

EP - 302

JO - Australian Journal of Chemistry

JF - Australian Journal of Chemistry

IS - 2

ER -

Crystal structure of 3, 3a΄, 5, 5΄-tetra-t-butyl- 2΄-(3, 5-di-t-butyl-4-hydroxyphenyl)- 7΄-[l-(3, 5-di-t-butyl-4-hydroxyphenyl)ethylidene]- 3a΄, 4΄, 7΄, 7a΄-tetrahydrospiro[cyclohexa- 2, 5-diene-1, 1΄-[1h]indene]-4, 4΄-dione

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