Crystal structure of (E)-7-t-Butyl-5-methoxy-3-[(E)-2'-methoxy-5',5'-dimethyl-4'-oxohex-2'-enylidene]benzofuran-2(3H)-one

Sydney R. Hall; Colin L. Raston; Allan H. White

doi:10.1071/CH9771979

Crystal structure of (E)-7-t-Butyl-5-methoxy-3-[(E)-2'-methoxy-5',5'-dimethyl-4'-oxohex-2'-enylidene]benzofuran-2(3H)-one

Sydney R. Hall, Colin L. Raston, Allan H. White

Research output: Contribution to journal › Article › peer-review

8 Citations (Scopus)

Abstract

The crystal structure of (E)-7-t-butyl-5-methoxy-3-[(E)-2'-methoxy- 5',5'-dimethyl-4'-oxohex-2‘enylidene]benzofuran-2(3H)-one, C₂₂H₂₈O₅ (see preceding paper), has been determined by single-crystal X-ray diffraction at 295(1) K and refined by least squares to a residual of 0.067 (3735 ‘observed’ reflections). Crystals are triclinic, PĪ, a 14.955(7), b 13.142(5), c 10.910(3) Å, α 85.76(3), β 85.67(3), γ 80.12(3)°, Z 4.

Original language	English
Pages (from-to)	1979-1986
Number of pages	8
Journal	Australian Journal of Chemistry
Volume	30
Issue number	9
DOIs	https://doi.org/10.1071/CH9771979
Publication status	Published - 1977
Externally published	Yes

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title = "Crystal structure of (E)-7-t-Butyl-5-methoxy-3-[(E)-2'-methoxy-5',5'-dimethyl-4'-oxohex-2'-enylidene]benzofuran-2(3H)-one",

abstract = "The crystal structure of (E)-7-t-butyl-5-methoxy-3-[(E)-2'-methoxy- 5',5'-dimethyl-4'-oxohex-2{\textquoteleft}enylidene]benzofuran-2(3H)-one, C22H28O5 (see preceding paper), has been determined by single-crystal X-ray diffraction at 295(1) K and refined by least squares to a residual of 0.067 (3735 {\textquoteleft}observed{\textquoteright} reflections). Crystals are triclinic, PĪ, a 14.955(7), b 13.142(5), c 10.910(3) {\AA}, α 85.76(3), β 85.67(3), γ 80.12(3)°, Z 4.",

author = "Hall, {Sydney R.} and Raston, {Colin L.} and White, {Allan H.}",

year = "1977",

doi = "10.1071/CH9771979",

language = "English",

volume = "30",

pages = "1979--1986",

journal = "Australian Journal of Chemistry",

issn = "0004-9425",

publisher = "CSIRO Publishing",

number = "9",

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T1 - Crystal structure of (E)-7-t-Butyl-5-methoxy-3-[(E)-2'-methoxy-5',5'-dimethyl-4'-oxohex-2'-enylidene]benzofuran-2(3H)-one

AU - Hall, Sydney R.

AU - Raston, Colin L.

AU - White, Allan H.

PY - 1977

Y1 - 1977

N2 - The crystal structure of (E)-7-t-butyl-5-methoxy-3-[(E)-2'-methoxy- 5',5'-dimethyl-4'-oxohex-2‘enylidene]benzofuran-2(3H)-one, C22H28O5 (see preceding paper), has been determined by single-crystal X-ray diffraction at 295(1) K and refined by least squares to a residual of 0.067 (3735 ‘observed’ reflections). Crystals are triclinic, PĪ, a 14.955(7), b 13.142(5), c 10.910(3) Å, α 85.76(3), β 85.67(3), γ 80.12(3)°, Z 4.

AB - The crystal structure of (E)-7-t-butyl-5-methoxy-3-[(E)-2'-methoxy- 5',5'-dimethyl-4'-oxohex-2‘enylidene]benzofuran-2(3H)-one, C22H28O5 (see preceding paper), has been determined by single-crystal X-ray diffraction at 295(1) K and refined by least squares to a residual of 0.067 (3735 ‘observed’ reflections). Crystals are triclinic, PĪ, a 14.955(7), b 13.142(5), c 10.910(3) Å, α 85.76(3), β 85.67(3), γ 80.12(3)°, Z 4.

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