TY - JOUR
T1 - Crystal structure of methyl 8-Iodo-4,5,7-trimethoxy-2-naphthoate
AU - Cameron, Donald W.
AU - Feutrill, Geoffrey I.
AU - Lammerts van Bueren, Lind J.H.
AU - Raston, Colin L.
AU - White, Allan H.
PY - 1977
Y1 - 1977
N2 - The crystal structure of the title compound, C15H15IO5, has been determined by single crystal X-ray diffraction at 295 K and refined by least squares to a residual of 0.04 (2210 ‘observed’ reflections). Crystals are monoclinic, P21/c, a 10.294(5), b 18.868(9), c 7.549(6) Å, β 90.29(5)°, Z 4. The molecular geometry apart from the iodine environment is as expected; the crystal packing is such that the iodine lies close to a symmetry-related neighbour at II 4.148(2) Å and may account for the observed facile elimination of iodine from the solid on heating to 120°C.
AB - The crystal structure of the title compound, C15H15IO5, has been determined by single crystal X-ray diffraction at 295 K and refined by least squares to a residual of 0.04 (2210 ‘observed’ reflections). Crystals are monoclinic, P21/c, a 10.294(5), b 18.868(9), c 7.549(6) Å, β 90.29(5)°, Z 4. The molecular geometry apart from the iodine environment is as expected; the crystal packing is such that the iodine lies close to a symmetry-related neighbour at II 4.148(2) Å and may account for the observed facile elimination of iodine from the solid on heating to 120°C.
UR - http://www.scopus.com/inward/record.url?scp=36749016048&partnerID=8YFLogxK
U2 - 10.1071/CH9772313
DO - 10.1071/CH9772313
M3 - Article
AN - SCOPUS:36749016048
VL - 30
SP - 2313
EP - 2317
JO - Australian Journal of Chemistry
JF - Australian Journal of Chemistry
SN - 0004-9425
IS - 10
ER -