Crystal structure of methyl 8-Iodo-4,5,7-trimethoxy-2-naphthoate

Donald W. Cameron, Geoffrey I. Feutrill, Lind J.H. Lammerts van Bueren, Colin L. Raston, Allan H. White

Research output: Contribution to journalArticle

5 Citations (Scopus)

Abstract

The crystal structure of the title compound, C15H15IO5, has been determined by single crystal X-ray diffraction at 295 K and refined by least squares to a residual of 0.04 (2210 ‘observed’ reflections). Crystals are monoclinic, P21/c, a 10.294(5), b 18.868(9), c 7.549(6) Å, β 90.29(5)°, Z 4. The molecular geometry apart from the iodine environment is as expected; the crystal packing is such that the iodine lies close to a symmetry-related neighbour at II 4.148(2) Å and may account for the observed facile elimination of iodine from the solid on heating to 120°C.

Original languageEnglish
Pages (from-to)2313-2317
Number of pages5
JournalAustralian Journal of Chemistry
Volume30
Issue number10
DOIs
Publication statusPublished - 1977
Externally publishedYes

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    Cameron, D. W., Feutrill, G. I., Lammerts van Bueren, L. J. H., Raston, C. L., & White, A. H. (1977). Crystal structure of methyl 8-Iodo-4,5,7-trimethoxy-2-naphthoate. Australian Journal of Chemistry, 30(10), 2313-2317. https://doi.org/10.1071/CH9772313