Crystal structure of Tetracyclo[5,3,1,12,6,04,9]dodecane (iceane)

David P.G. Hamon; Colin L. Raston; Garry F. Taylor; Jose N. Varghese; Allan H. White

doi:10.1071/CH9771837

Crystal structure of Tetracyclo[5,3,1,1^2,6,0^4,9]dodecane (iceane)

David P.G. Hamon, Colin L. Raston, Garry F. Taylor, Jose N. Varghese, Allan H. White

Research output: Contribution to journal › Article › peer-review

8 Citations (Scopus)

Abstract

The crystal structure of the title compound, C₁₂H₁₈, has been determined at 295 K by X-ray diffraction and refined by full-matrix least squares to a residual of 0.049 for 216 ‘observed’ reflections; molecular geometry has been corrected for the effects of thermal motion using a rigid body approximation. Crystals are hexagonal, P63/m, a = 6.582(1), c = 11.843(3) Å, Z = 2, the molecules occupying a hexagonal close-packed array.

Original language	English
Pages (from-to)	1837-1840
Number of pages	4
Journal	Australian Journal of Chemistry
Volume	30
Issue number	8
DOIs	https://doi.org/10.1071/CH9771837
Publication status	Published - 1977
Externally published	Yes

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title = "Crystal structure of Tetracyclo[5,3,1,12,6,04,9]dodecane (iceane)",

abstract = "The crystal structure of the title compound, C12H18, has been determined at 295 K by X-ray diffraction and refined by full-matrix least squares to a residual of 0.049 for 216 {\textquoteleft}observed{\textquoteright} reflections; molecular geometry has been corrected for the effects of thermal motion using a rigid body approximation. Crystals are hexagonal, P63/m, a = 6.582(1), c = 11.843(3) {\AA}, Z = 2, the molecules occupying a hexagonal close-packed array.",

author = "Hamon, {David P.G.} and Raston, {Colin L.} and Taylor, {Garry F.} and Varghese, {Jose N.} and White, {Allan H.}",

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AU - Hamon, David P.G.

AU - Raston, Colin L.

AU - Taylor, Garry F.

AU - Varghese, Jose N.

AU - White, Allan H.

PY - 1977

Y1 - 1977

N2 - The crystal structure of the title compound, C12H18, has been determined at 295 K by X-ray diffraction and refined by full-matrix least squares to a residual of 0.049 for 216 ‘observed’ reflections; molecular geometry has been corrected for the effects of thermal motion using a rigid body approximation. Crystals are hexagonal, P63/m, a = 6.582(1), c = 11.843(3) Å, Z = 2, the molecules occupying a hexagonal close-packed array.

AB - The crystal structure of the title compound, C12H18, has been determined at 295 K by X-ray diffraction and refined by full-matrix least squares to a residual of 0.049 for 216 ‘observed’ reflections; molecular geometry has been corrected for the effects of thermal motion using a rigid body approximation. Crystals are hexagonal, P63/m, a = 6.582(1), c = 11.843(3) Å, Z = 2, the molecules occupying a hexagonal close-packed array.

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Crystal structure of Tetracyclo[5,3,1,1^2,6,0^4,9]dodecane (iceane)

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