The crystal structure of the title compound has been determined by the heavy-atom method from X-ray diffractometer data, and refined by full-matrix least-squares to R 0.064 for 3 292 observed reflections. Crystals are monoclinic, space group C2/c, and isostructural with the cobalt(III) analogue: a = 14.071(5), b = 10.477(3), c = 16.980(5) Å, β = 108.61 (2)°, Z = 4. Mean Ir-S is 2.367 Å.
|Number of pages||4|
|Journal||Journal of the Chemical Society, Dalton Transactions|
|Publication status||Published - 1976|