TY - JOUR
T1 - Crystal structure of tris(NN-diethyldithiocarbamato)iron(IV) pentaiodide
AU - Raston, Colin L.
AU - White, Allan H.
AU - Petridis, Dimitris
AU - Taylor, Donald
PY - 1980
Y1 - 1980
N2 - The crystal structure of the title compound [Fe(S2CNEt2)3][I5], has been determined by X-ray diffraction at 295(1) K, being refined to a residual of 0.049 for 3 328 'observed' reflections. Crystals are triclinic, space group P1, a = 17.41(1), b = 10.197(9), c = 10.184(8) Å, α = 74.71(6), β = 73.29(6), γ = 89.19(7)°, and Z = 2. The structure comprises [Fe(S2CNEt2)3]+ cations and I5- anions. Within the cation the symmetry is approximately D3 with six Fe-S distances ranging between 2.292(4) and 2.314(4) Å.
AB - The crystal structure of the title compound [Fe(S2CNEt2)3][I5], has been determined by X-ray diffraction at 295(1) K, being refined to a residual of 0.049 for 3 328 'observed' reflections. Crystals are triclinic, space group P1, a = 17.41(1), b = 10.197(9), c = 10.184(8) Å, α = 74.71(6), β = 73.29(6), γ = 89.19(7)°, and Z = 2. The structure comprises [Fe(S2CNEt2)3]+ cations and I5- anions. Within the cation the symmetry is approximately D3 with six Fe-S distances ranging between 2.292(4) and 2.314(4) Å.
UR - http://www.scopus.com/inward/record.url?scp=37049103498&partnerID=8YFLogxK
U2 - 10.1039/DT9800001928
DO - 10.1039/DT9800001928
M3 - Article
AN - SCOPUS:37049103498
SN - 1472-7773
SP - 1928
EP - 1931
JO - Journal of the Chemical Society. Dalton Transactions
JF - Journal of the Chemical Society. Dalton Transactions
IS - 10
ER -