Crystal structure of (Z)-Cembr-4-ene-15,19,20-triol

Edward N. Maslen; Colin L. Raston; Allan H. White

doi:10.1071/CH9772723

Crystal structure of (Z)-Cembr-4-ene-15,19,20-triol

Edward N. Maslen, Colin L. Raston, Allan H. White

Research output: Contribution to journal › Article › peer-review

3 Citations (Scopus)

Abstract

The crystal structure of the title compound, CZOH3803 [compound (1) in ref.'], has been determined by single-crystal X-ray diffraction at 295(1) K and refined by least squares to a residual of 0.045 for 954 ‘observed’ reflections. Crystals are monoclinic, P2', a 9.281(2), b 17.798(6), c 6.417(1) A, B 93.81(3)', Z 2. The structure determination establishes the relative configuration of the chiral centres within the 14-membered macrocyclic ring and shows the double bond to have the unusual (Z) configuration.

Original language	English
Pages (from-to)	2723-2727
Number of pages	5
Journal	Australian Journal of Chemistry
Volume	30
Issue number	12
DOIs	https://doi.org/10.1071/CH9772723
Publication status	Published - 1977
Externally published	Yes

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title = "Crystal structure of (Z)-Cembr-4-ene-15,19,20-triol",

abstract = "The crystal structure of the title compound, CZOH3803 [compound (1) in ref.'], has been determined by single-crystal X-ray diffraction at 295(1) K and refined by least squares to a residual of 0.045 for 954 {\textquoteleft}observed{\textquoteright} reflections. Crystals are monoclinic, P2', a 9.281(2), b 17.798(6), c 6.417(1) A, B 93.81(3)', Z 2. The structure determination establishes the relative configuration of the chiral centres within the 14-membered macrocyclic ring and shows the double bond to have the unusual (Z) configuration.",

author = "Maslen, {Edward N.} and Raston, {Colin L.} and White, {Allan H.}",

year = "1977",

doi = "10.1071/CH9772723",

language = "English",

volume = "30",

pages = "2723--2727",

journal = "Australian Journal of Chemistry",

issn = "0004-9425",

publisher = "CSIRO Publishing",

number = "12",

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T1 - Crystal structure of (Z)-Cembr-4-ene-15,19,20-triol

AU - Maslen, Edward N.

AU - Raston, Colin L.

AU - White, Allan H.

PY - 1977

Y1 - 1977

N2 - The crystal structure of the title compound, CZOH3803 [compound (1) in ref.'], has been determined by single-crystal X-ray diffraction at 295(1) K and refined by least squares to a residual of 0.045 for 954 ‘observed’ reflections. Crystals are monoclinic, P2', a 9.281(2), b 17.798(6), c 6.417(1) A, B 93.81(3)', Z 2. The structure determination establishes the relative configuration of the chiral centres within the 14-membered macrocyclic ring and shows the double bond to have the unusual (Z) configuration.

AB - The crystal structure of the title compound, CZOH3803 [compound (1) in ref.'], has been determined by single-crystal X-ray diffraction at 295(1) K and refined by least squares to a residual of 0.045 for 954 ‘observed’ reflections. Crystals are monoclinic, P2', a 9.281(2), b 17.798(6), c 6.417(1) A, B 93.81(3)', Z 2. The structure determination establishes the relative configuration of the chiral centres within the 14-membered macrocyclic ring and shows the double bond to have the unusual (Z) configuration.

UR - http://www.scopus.com/inward/record.url?scp=84970541477&partnerID=8YFLogxK

U2 - 10.1071/CH9772723

DO - 10.1071/CH9772723

M3 - Article

AN - SCOPUS:84970541477

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VL - 30

SP - 2723

EP - 2727

JO - Australian Journal of Chemistry

JF - Australian Journal of Chemistry

IS - 12

ER -

Crystal structure of (Z)-Cembr-4-ene-15,19,20-triol

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