TY - JOUR
T1 - Preparation of N-(Pyrrol-1-yl)maleimide and 5-(Pyrrol-1-y1imino)furan-2(5H)-one
T2 - Crystal Structure of 2-(Pyrrol-1-yl)-4, 7-dihydro-4, 7-epoxyisoindole-1, 3(7aH, 3aH)-dione
AU - Diakiw, Vladimir
AU - Raston, Colin L.
AU - Stewart, Murray
AU - White, Allan H.
PY - 1978/1/1
Y1 - 1978/1/1
N2 - The synthesis and some properties of N-(pyrrol-1-yl)maleimide (1) and its isomer (6) are described. The structure of 2-(pyrrol-1-yl)-4, 7-dihydro-4, 7-epoxyisoindole-l, 3(7aH, 3aH)-dione (8), a key intermediate in the synthesis of (1), has been determined by single-crystal X-ray diffraction at 298 K, and refined by least squares to a residual of 0·046 for 1977 'observed' reflections. Crystals are tri-clinic, P1, a 8·472(5), b 10·130(6), c 12·760(8) Å, α 91·12(5), β 92·09(5), γ 102·90(4)°, Z 4.
AB - The synthesis and some properties of N-(pyrrol-1-yl)maleimide (1) and its isomer (6) are described. The structure of 2-(pyrrol-1-yl)-4, 7-dihydro-4, 7-epoxyisoindole-l, 3(7aH, 3aH)-dione (8), a key intermediate in the synthesis of (1), has been determined by single-crystal X-ray diffraction at 298 K, and refined by least squares to a residual of 0·046 for 1977 'observed' reflections. Crystals are tri-clinic, P1, a 8·472(5), b 10·130(6), c 12·760(8) Å, α 91·12(5), β 92·09(5), γ 102·90(4)°, Z 4.
UR - http://www.scopus.com/inward/record.url?scp=84970593874&partnerID=8YFLogxK
U2 - 10.1071/CH9781021
DO - 10.1071/CH9781021
M3 - Article
AN - SCOPUS:84970593874
VL - 31
SP - 1021
EP - 1029
JO - Australian Journal of Chemistry
JF - Australian Journal of Chemistry
SN - 0004-9425
IS - 5
ER -