Synthesis of 2-imino-5-phenylimidazolidin-4-one and the structure of its trifluoroacetate salt

Jerry L. Atwood; Leonard J. Barbour; Michael W. Heaven; Colin L. Raston

doi:10.1023/A:1023545425398

Synthesis of 2-imino-5-phenylimidazolidin-4-one and the structure of its trifluoroacetate salt

Jerry L. Atwood, Leonard J. Barbour, Michael W. Heaven, Colin L. Raston

Research output: Contribution to journal › Article › peer-review

3 Citations (Scopus)

Abstract

The trifluoroacetate salt of 2-imino-5-phenylimidazolidin-4-one has been prepared and characterized crystallographically. The complex crystallizes in the monoclinic space group C2, with a = 27.894(3) Å, b = 6.2616(7) Å, c = 7.1989(8) Å, β = 93.176(2)°. The extended structure consists of neutral, one-dimensional, hydrogen-bonded ribbons incorporating both ionic species.

Original language	English
Pages (from-to)	175-179
Number of pages	5
Journal	Journal of Chemical Crystallography
Volume	33
Issue number	3
DOIs	https://doi.org/10.1023/A:1023545425398
Publication status	Published - 1 Mar 2003
Externally published	Yes

Keywords

Crystal structure
Glycoluril
Guanidine
Hydrogen bonding

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title = "Synthesis of 2-imino-5-phenylimidazolidin-4-one and the structure of its trifluoroacetate salt",

abstract = "The trifluoroacetate salt of 2-imino-5-phenylimidazolidin-4-one has been prepared and characterized crystallographically. The complex crystallizes in the monoclinic space group C2, with a = 27.894(3) {\AA}, b = 6.2616(7) {\AA}, c = 7.1989(8) {\AA}, β = 93.176(2)°. The extended structure consists of neutral, one-dimensional, hydrogen-bonded ribbons incorporating both ionic species.",

keywords = "Crystal structure, Glycoluril, Guanidine, Hydrogen bonding",

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T1 - Synthesis of 2-imino-5-phenylimidazolidin-4-one and the structure of its trifluoroacetate salt

AU - Atwood, Jerry L.

AU - Barbour, Leonard J.

AU - Heaven, Michael W.

AU - Raston, Colin L.

PY - 2003/3/1

Y1 - 2003/3/1

N2 - The trifluoroacetate salt of 2-imino-5-phenylimidazolidin-4-one has been prepared and characterized crystallographically. The complex crystallizes in the monoclinic space group C2, with a = 27.894(3) Å, b = 6.2616(7) Å, c = 7.1989(8) Å, β = 93.176(2)°. The extended structure consists of neutral, one-dimensional, hydrogen-bonded ribbons incorporating both ionic species.

AB - The trifluoroacetate salt of 2-imino-5-phenylimidazolidin-4-one has been prepared and characterized crystallographically. The complex crystallizes in the monoclinic space group C2, with a = 27.894(3) Å, b = 6.2616(7) Å, c = 7.1989(8) Å, β = 93.176(2)°. The extended structure consists of neutral, one-dimensional, hydrogen-bonded ribbons incorporating both ionic species.

KW - Crystal structure

KW - Glycoluril

KW - Guanidine

KW - Hydrogen bonding

UR - http://www.scopus.com/inward/record.url?scp=0038365254&partnerID=8YFLogxK

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DO - 10.1023/A:1023545425398

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EP - 179

JO - Journal of Chemical Crystallography

JF - Journal of Chemical Crystallography

IS - 3

ER -

Synthesis of 2-imino-5-phenylimidazolidin-4-one and the structure of its trifluoroacetate salt

Abstract

Keywords

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