The Chemistry of Dodonaea spp. VIII Isolation and Crystal Structure of a Diterpene Acid from Dodonaea petiolaris

Phillip R. Jefferies; Trevor G. Payne; Colin L. Raston; Allan H. White

doi:10.1071/CH9811001

The Chemistry of Dodonaea spp. VIII Isolation and Crystal Structure of a Diterpene Acid from Dodonaea petiolaris

Phillip R. Jefferies
, Trevor G. Payne
, Colin L. Raston
, Allan H. White

Research output: Contribution to journal › Article › peer-review

9 Citations (Scopus)

Abstract

On the basis of physical data, an acid isolated from the title plant is found to be ent-3ß-acetoxy- 15, 16-epoxylabda-8(17), 13(16), 14-trien-18-oic acid (1) or its enantiomer. The crystal structure of the acid, C22H2806, was determined from single-crystal diffractometer data at 295(1) K, being refined by least squares to a residual of 0•056 for 922 ‘observed’ reflections; crystals are orthorhombic, P2 ₁ 2 ₁ 2 ₁ , a 16•22(1), b 12•212(5), c 9•976(3) Å, Z 4.

Original language	English
Pages (from-to)	1001-1007
Number of pages	7
Journal	Australian Journal of Chemistry
Volume	34
Issue number	5
DOIs	https://doi.org/10.1071/CH9811001
Publication status	Published - 1981
Externally published	Yes

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title = "The Chemistry of Dodonaea spp. VIII Isolation and Crystal Structure of a Diterpene Acid from Dodonaea petiolaris",

abstract = " On the basis of physical data, an acid isolated from the title plant is found to be ent-3{\ss}-acetoxy- 15, 16-epoxylabda-8(17), 13(16), 14-trien-18-oic acid (1) or its enantiomer. The crystal structure of the acid, C22H2806, was determined from single-crystal diffractometer data at 295(1) K, being refined by least squares to a residual of 0•056 for 922 {\textquoteleft}observed{\textquoteright} reflections; crystals are orthorhombic, P2 1 2 1 2 1 , a 16•22(1), b 12•212(5), c 9•976(3) {\AA}, Z 4.",

author = "Jefferies, \{Phillip R.\} and Payne, \{Trevor G.\} and Raston, \{Colin L.\} and White, \{Allan H.\}",

year = "1981",

doi = "10.1071/CH9811001",

language = "English",

volume = "34",

pages = "1001--1007",

journal = "Australian Journal of Chemistry",

issn = "0004-9425",

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T1 - The Chemistry of Dodonaea spp. VIII Isolation and Crystal Structure of a Diterpene Acid from Dodonaea petiolaris

AU - Jefferies, Phillip R.

AU - Payne, Trevor G.

AU - Raston, Colin L.

AU - White, Allan H.

PY - 1981

Y1 - 1981

N2 - On the basis of physical data, an acid isolated from the title plant is found to be ent-3ß-acetoxy- 15, 16-epoxylabda-8(17), 13(16), 14-trien-18-oic acid (1) or its enantiomer. The crystal structure of the acid, C22H2806, was determined from single-crystal diffractometer data at 295(1) K, being refined by least squares to a residual of 0•056 for 922 ‘observed’ reflections; crystals are orthorhombic, P2 1 2 1 2 1 , a 16•22(1), b 12•212(5), c 9•976(3) Å, Z 4.

AB - On the basis of physical data, an acid isolated from the title plant is found to be ent-3ß-acetoxy- 15, 16-epoxylabda-8(17), 13(16), 14-trien-18-oic acid (1) or its enantiomer. The crystal structure of the acid, C22H2806, was determined from single-crystal diffractometer data at 295(1) K, being refined by least squares to a residual of 0•056 for 922 ‘observed’ reflections; crystals are orthorhombic, P2 1 2 1 2 1 , a 16•22(1), b 12•212(5), c 9•976(3) Å, Z 4.

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SN - 0004-9425

VL - 34

SP - 1001

EP - 1007

JO - Australian Journal of Chemistry

JF - Australian Journal of Chemistry

IS - 5

ER -

The Chemistry of Dodonaea spp. VIII Isolation and Crystal Structure of a Diterpene Acid from Dodonaea petiolaris

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